The limits of quantification (LOQs) reached were lower than 0.2 μg kg −1 in apple (0.2 μg L −1 apple juice) in most cases. Recoveries were between 70–120% and two ranges of linearity were observed: 0.5–20 μg kg −1 (0.5–20 μg L −1 apple juice) and 20–100 μg kg −1 (20–100 μg L −1 apple juice). Trueness, precision, linearity, and robustness values were validated in raw fruit (apple) and juice (apple juice) as representative solid and liquid food commodities. The target approach has been validated according to SANTE Guide requirements. A new polyvalent wide-scope analytical method, valid for both raw and processed (juices) fruits, combining target and non-target strategies, has been developed and validated to determine low concentrations of 260 pesticides, as well as many potential non-target substances and metabolites.
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